Porosimetry

The Micromeritics Autopore IV 9500 has one high-pressure port and two low-pressure ports. Due to the use of elemental mercury, only the MSE technician operates the instrument. Data is collected and analyzed via a windows XP environment. Samples should be dried in a 50C-drying oven 24 hours before the measurement is made. Please give 24 hours notice before scheduling an appointment. Please use the link provided for more technical information.
Technical Information

Low Pressure:
Measurement: 0 - 30 psi
Resolution: 0.01 psi
Pore Diameter: 360 - 3.6 um
Transducer Accuracy: +/- 1% of full scale

High Pressure:
Measurement: 30 - 30,000 psi
Resolution: atm - 3000psi - 0.1 psi
3000 - 30,000psi - 0.2 psi
Pore diameter: 6 - 0.005um
Transducer Accuracy: +/- 1% of full scale

Intrusion:
Resolution: Better than 0.1 uL
Accuracy: +/- 1% of max pen stem volume

Penetrometers:
Capillary Stem Intrusion Volumes: 0.38, 1.1, 1.7, 3.1, and 3.9 cm^3.

Sample size:
Max: a cylinder 2.5 cm diameter by 2.5 cm long.

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