{"id":1865,"date":"2017-09-28T12:09:17","date_gmt":"2017-09-28T19:09:17","guid":{"rendered":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/?p=1865"},"modified":"2017-09-28T12:09:17","modified_gmt":"2017-09-28T19:09:17","slug":"update-av500-probe-changed-to-triple-resonance-hcp","status":"publish","type":"post","link":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/2017\/09\/update-av500-probe-changed-to-triple-resonance-hcp\/","title":{"rendered":"UPDATE ! AV500 &#8211; PROBE CHANGED TO TRIPLE RESONANCE &#8211; HCP"},"content":{"rendered":"<p>The BBI probe&#8217;s VT dewar is faulty, which most probably contributed to an over temperature event.\u00a0 Since we have to wait for the replacement part to arrive (might be a couple of weeks), the following probehead has been placed and optimized for regular use :<\/p>\n<p><strong>TXI &#8211; 1H {13C, 31P) &#8211; XYZ gradient<\/strong><\/p>\n<ul>\n<li>This probe is designed for best 1H sensitivity, similar to the BBI probe that came out.<\/li>\n<li>In the default configuration you can run 13C NMR without any modifications.<\/li>\n<li>If you want to run 31P, you have to pull the RF cable connected to 13C and connect it to the 31P connector on the probe &#8211; similar to what you will do with the TXO &#8211; 19F\u00a0 probe in DRX499.<\/li>\n<li>You can use Topshim as before.<\/li>\n<li>The low temperature rnage of this probe is limited &#8211; a nominal value of -40 C is available for now. \u00a0 If you want to go lower than this, please contact me or Adrienne.<\/li>\n<li>The high temperature limit is +70 C, as before.<\/li>\n<\/ul>\n<p>Please contact, if you have further questions.<\/p>\n<p>NMR Facility Manager<\/p>\n<p>9\/28\/2017<\/p>\n","protected":false},"excerpt":{"rendered":"<p>The BBI probe&#8217;s VT dewar is faulty, which most probably contributed to an over temperature event.\u00a0 Since we have to wait for the replacement part to arrive (might be a couple of weeks), the following probehead has been placed and optimized for regular use : TXI &#8211; 1H {13C, 31P) &#8211; XYZ gradient This probe [&hellip;]<\/p>\n","protected":false},"author":19,"featured_media":0,"comment_status":"open","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":[],"categories":[11,9],"tags":[],"_links":{"self":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/1865"}],"collection":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/users\/19"}],"replies":[{"embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/comments?post=1865"}],"version-history":[{"count":1,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/1865\/revisions"}],"predecessor-version":[{"id":1866,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/1865\/revisions\/1866"}],"wp:attachment":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/media?parent=1865"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/categories?post=1865"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/tags?post=1865"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}