{"id":1954,"date":"2018-04-11T09:01:35","date_gmt":"2018-04-11T16:01:35","guid":{"rendered":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/?p=1954"},"modified":"2018-04-11T09:01:35","modified_gmt":"2018-04-11T16:01:35","slug":"av700-solids-nmr-usage-brief-clarification","status":"publish","type":"post","link":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/2018\/04\/av700-solids-nmr-usage-brief-clarification\/","title":{"rendered":"AV700 SOLIDS NMR USAGE :  BRIEF CLARIFICATION"},"content":{"rendered":"<p>Unlike the solutions spectrometers,\u00a0 solid state NMR instrument is not amenable to a walk-on mode of operation, by the very nature of this spectroscopy.\u00a0\u00a0 First of all, the technique requires the use of an expensive rotor (approx. cost $1000\/- ) in place of the NMR tube that costs about $10\/-.\u00a0 The sample preparation also needs to be carefully performed since the rotor spins at rates of 15 kHz or more.\u00a0\u00a0 Last but not least, acquisition of even the rudimentary spectra requires, hours if not days of spectrometer time.<\/p>\n<p>For these reasons, every run requires a bit of hand holding and guidance, within the purview of available capabilities in our facility.<\/p>\n<p>To further explore the technique and see if your research will uniquely benefit from this special tool, please contact Adrienne Roehrich.<\/p>\n<p>NMR Facility Manager<\/p>\n<p>4\/11\/2018<\/p>\n","protected":false},"excerpt":{"rendered":"<p>Unlike the solutions spectrometers,\u00a0 solid state NMR instrument is not amenable to a walk-on mode of operation, by the very nature of this spectroscopy.\u00a0\u00a0 First of all, the technique requires the use of an expensive rotor (approx. cost $1000\/- ) in place of the NMR tube that costs about $10\/-.\u00a0 The sample preparation also needs [&hellip;]<\/p>\n","protected":false},"author":19,"featured_media":0,"comment_status":"open","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":[],"categories":[10,9,7],"tags":[],"_links":{"self":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/1954"}],"collection":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/users\/19"}],"replies":[{"embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/comments?post=1954"}],"version-history":[{"count":1,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/1954\/revisions"}],"predecessor-version":[{"id":1955,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/1954\/revisions\/1955"}],"wp:attachment":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/media?parent=1954"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/categories?post=1954"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/tags?post=1954"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}