{"id":2093,"date":"2018-09-27T17:47:35","date_gmt":"2018-09-28T00:47:35","guid":{"rendered":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/?p=2093"},"modified":"2018-09-27T17:47:35","modified_gmt":"2018-09-28T00:47:35","slug":"update-av300-system-back-to-normal","status":"publish","type":"post","link":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/2018\/09\/update-av300-system-back-to-normal\/","title":{"rendered":"UPDATE ! AV300 : SYSTEM BACK TO NORMAL"},"content":{"rendered":"<ul>\n<li><strong>1H ACQUISITION <\/strong> Works as expected.\u00a0 Pulse width is already optimized. If you are in doubt you should run command &#8220;<strong>getprosol&#8221;.<\/strong><\/li>\n<li><strong>X ACQUISITION (13C, etc.)<\/strong> Works as expected.\u00a0 You might notice an increased noise level if you happen to run the spectrum on a previous sample for which you have data and compare it.\u00a0\u00a0 <strong>The 90 pulse width for Carbon is not optimized yet,<\/strong> along with the change in the hardware conditions. This is one important cause of the above.\u00a0 (Will update once this is taken care of).<\/li>\n<li><strong>TOPSHIM ON 2H LOCK SOLVENTS : <\/strong>Works as expected.\u00a0\u00a0 I had access to only a few organic solvents to test it out.\u00a0 If you happen to use a less frequent solvent and face issues, <strong>please contact me immediately. <\/strong><\/li>\n<\/ul>\n<p>Thank you for your patience.<\/p>\n<p>NMR Facility Manager<\/p>\n<p>9\/27\/18<\/p>\n","protected":false},"excerpt":{"rendered":"<p>1H ACQUISITION Works as expected.\u00a0 Pulse width is already optimized. If you are in doubt you should run command &#8220;getprosol&#8221;. X ACQUISITION (13C, etc.) Works as expected.\u00a0 You might notice an increased noise level if you happen to run the spectrum on a previous sample for which you have data and compare it.\u00a0\u00a0 The 90 [&hellip;]<\/p>\n","protected":false},"author":19,"featured_media":0,"comment_status":"open","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":[],"categories":[11,9],"tags":[],"_links":{"self":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/2093"}],"collection":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/users\/19"}],"replies":[{"embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/comments?post=2093"}],"version-history":[{"count":1,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/2093\/revisions"}],"predecessor-version":[{"id":2094,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/2093\/revisions\/2094"}],"wp:attachment":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/media?parent=2093"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/categories?post=2093"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/tags?post=2093"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}