{"id":2115,"date":"2018-11-27T15:31:37","date_gmt":"2018-11-27T23:31:37","guid":{"rendered":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/?p=2115"},"modified":"2018-11-27T15:31:37","modified_gmt":"2018-11-27T23:31:37","slug":"alert-av500-new-tbi-probe-is-ready-for-use","status":"publish","type":"post","link":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/2018\/11\/alert-av500-new-tbi-probe-is-ready-for-use\/","title":{"rendered":"ALERT !  AV500 &#8211; NEW TBI PROBE IS READY FOR USE"},"content":{"rendered":"<p>Triple Resonance probe <strong>TBI &#8211; 1H, 13C {X-BB}-Z gradient probe <\/strong>is ready for use.<\/p>\n<p><em><strong>STANDARD SHIM SET :\u00a0<\/strong><\/em> <strong>Please start with &#8216;rsh stdtbi&#8217;\u00a0 and proceed with Topshim.\u00a0\u00a0 Of course, you have to lock onto your solvent first.<\/strong><\/p>\n<p>Few highlights about the probe:<\/p>\n<ul>\n<li>Here is the front plate view that is self-explanatory<\/li>\n<\/ul>\n<div id=\"attachment_2114\" style=\"width: 634px\" class=\"wp-caption alignnone\"><a href=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2018\/11\/TBI_front_view.jpg\"><img aria-describedby=\"caption-attachment-2114\" decoding=\"async\" loading=\"lazy\" class=\"wp-image-2114 size-large\" src=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2018\/11\/TBI_front_view-e1543360534932-768x1024.jpg\" alt=\"\" width=\"624\" height=\"832\" srcset=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2018\/11\/TBI_front_view-e1543360534932-768x1024.jpg 768w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2018\/11\/TBI_front_view-e1543360534932-225x300.jpg 225w\" sizes=\"(max-width: 624px) 100vw, 624px\" \/><\/a><p id=\"caption-attachment-2114\" class=\"wp-caption-text\">1H and 13C have dedicated channels. Broadband (BB) channel is tuned to 31P normally. Can be changed according to the X nucleus observed. 2H NMR can be run without touching any cable.<\/p><\/div>\n<p>&nbsp;<\/p>\n<ul>\n<li>View of the Tune\/Match rods for 1H and 13C channels\n<p><div id=\"attachment_2113\" style=\"width: 634px\" class=\"wp-caption alignnone\"><a href=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2018\/11\/TBI_1H_13C_tune_match.jpg\"><img aria-describedby=\"caption-attachment-2113\" decoding=\"async\" loading=\"lazy\" class=\"size-large wp-image-2113\" src=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2018\/11\/TBI_1H_13C_tune_match-1024x778.jpg\" alt=\"\" width=\"624\" height=\"474\" srcset=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2018\/11\/TBI_1H_13C_tune_match-1024x778.jpg 1024w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2018\/11\/TBI_1H_13C_tune_match-300x228.jpg 300w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2018\/11\/TBI_1H_13C_tune_match-768x584.jpg 768w\" sizes=\"(max-width: 624px) 100vw, 624px\" \/><\/a><p id=\"caption-attachment-2113\" class=\"wp-caption-text\">The knobs rotate to adjust the resonance frequency. Inverted screw driver tool hangs by the side of these in a chain.<\/p><\/div><\/li>\n<li><strong>X<\/strong> a.k.a. <strong>Broadband channel <\/strong>tune and match paddles are shown here.\u00a0 By default, this channel is tuned and ready for <strong>31P <\/strong>observation (this is the third most popular nucleus after 1H and 13C).\u00a0\u00a0\u00a0 <strong><em>The most significant digit of the Match paddle is damaged. For most of the nuclei encountered, this won&#8217;t be a critical constraint. We will replace this as soon as possible. <a id=\"_idgpn_3\" href=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2018\/11\/XBB_tune_match_annotated.jpg\"><img decoding=\"async\" loading=\"lazy\" class=\"alignnone size-large wp-image-2112\" src=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2018\/11\/XBB_tune_match_annotated-961x1024.jpg\" alt=\"\" width=\"624\" height=\"665\" srcset=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2018\/11\/XBB_tune_match_annotated-961x1024.jpg 961w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2018\/11\/XBB_tune_match_annotated-282x300.jpg 282w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2018\/11\/XBB_tune_match_annotated-768x818.jpg 768w\" sizes=\"(max-width: 624px) 100vw, 624px\" \/><\/a><\/em><\/strong><\/li>\n<\/ul>\n<p>&nbsp;<\/p>\n<ul>\n<li><strong>You can use the default macros such as &#8216;proton&#8217; or &#8216;carbon&#8217; as before.\u00a0 This will load the standard shim set as well as pulse parameters. <\/strong><\/li>\n<li><strong>With the default configuration, 90% of the users can simply run spectra with minimal need for tuning\/matching i.e. 1H, 13C and 31P that is ready to go. <\/strong><\/li>\n<\/ul>\n<hr \/>\n<p><strong><span style=\"color: #ff0000;\">I will communicate with you more updates on this Probehead as well as the AV500 system itself, as we get closer to deploying the DRX499 for regular use.<\/span> <\/strong><\/p>\n<hr \/>\n<p>Stay Tuned<\/p>\n<p>NMR Facility Manager<\/p>\n<p>11\/27\/2018<\/p>\n<p><input id=\"idg-io-safe-browsing-enabled\" type=\"hidden\" \/><\/p>\n","protected":false},"excerpt":{"rendered":"<p>Triple Resonance probe TBI &#8211; 1H, 13C {X-BB}-Z gradient probe is ready for use. STANDARD SHIM SET :\u00a0 Please start with &#8216;rsh stdtbi&#8217;\u00a0 and proceed with Topshim.\u00a0\u00a0 Of course, you have to lock onto your solvent first. Few highlights about the probe: Here is the front plate view that is self-explanatory &nbsp; View of the [&hellip;]<\/p>\n","protected":false},"author":19,"featured_media":0,"comment_status":"open","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":[],"categories":[1],"tags":[],"_links":{"self":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/2115"}],"collection":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/users\/19"}],"replies":[{"embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/comments?post=2115"}],"version-history":[{"count":2,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/2115\/revisions"}],"predecessor-version":[{"id":2117,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/2115\/revisions\/2117"}],"wp:attachment":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/media?parent=2115"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/categories?post=2115"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/tags?post=2115"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}