{"id":2689,"date":"2022-09-21T17:40:25","date_gmt":"2022-09-22T00:40:25","guid":{"rendered":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/?p=2689"},"modified":"2022-09-21T17:40:25","modified_gmt":"2022-09-22T00:40:25","slug":"av301-system-ready-for-use-with-surrogate-bbi-probe","status":"publish","type":"post","link":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/2022\/09\/av301-system-ready-for-use-with-surrogate-bbi-probe\/","title":{"rendered":"AV301 : SYSTEM READY FOR USE WITH SURROGATE BBI PROBE"},"content":{"rendered":"<p>Dear Users<\/p>\n<h3>\u00a0\u00a0\u00a0\u00a0\u00a0 The regular probe with a faulty ATMA motor assembly is pulled out for repairs.\u00a0 <em>Do not underestimate the probe that is placed in the magnet as a backup, because it is called Surrogate.<\/em><\/h3>\n<p>This is a newly procured &#8220;gently used probe&#8221; in excellent condition and gives beautiful spectra as I show below.<\/p>\n<ul>\n<li>This is an <strong>inverse probehead, <\/strong>which means that it has the best sensitivity for 1H observation.<\/li>\n<li>You can also observe other nuclei, such as 13C, as you would have done with the PABBI probe<\/li>\n<li><strong>IMPORTANT :\u00a0 YOU HAVE TO TUNE\/MATCH THE PROBE BY HAND<\/strong><\/li>\n<\/ul>\n<p>Here is the Intro Card for the probe placed on the console : <a href=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BakBBI_card.jpeg\"><img decoding=\"async\" loading=\"lazy\" class=\"alignnone size-large wp-image-2684\" src=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BakBBI_card-1024x768.jpeg\" alt=\"\" width=\"624\" height=\"468\" srcset=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BakBBI_card-1024x768.jpeg 1024w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BakBBI_card-300x225.jpeg 300w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BakBBI_card-768x576.jpeg 768w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BakBBI_card.jpeg 2048w\" sizes=\"(max-width: 624px) 100vw, 624px\" \/><\/a><\/p>\n<p>&nbsp;<\/p>\n<p>The probe tunes great and I will show an example of the 13C channel Wobb curve.<a href=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BackupBBI_13C_wobb.png\"><img decoding=\"async\" loading=\"lazy\" class=\"alignnone  wp-image-2688\" src=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BackupBBI_13C_wobb-1024x760.png\" alt=\"\" width=\"610\" height=\"452\" srcset=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BackupBBI_13C_wobb-1024x760.png 1024w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BackupBBI_13C_wobb-300x223.png 300w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BackupBBI_13C_wobb-768x570.png 768w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BackupBBI_13C_wobb.png 1078w\" sizes=\"(max-width: 610px) 100vw, 610px\" \/><\/a><\/p>\n<p>Here is a 1H spectrum from Lineshape standard, highlighting the resolution seen with the Acetone-d6 pentet. <a href=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BackupBBI_lineshape_acetone.png\"><img decoding=\"async\" loading=\"lazy\" class=\"alignnone size-large wp-image-2687\" src=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BackupBBI_lineshape_acetone-1024x765.png\" alt=\"\" width=\"624\" height=\"466\" srcset=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BackupBBI_lineshape_acetone-1024x765.png 1024w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BackupBBI_lineshape_acetone-300x224.png 300w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BackupBBI_lineshape_acetone-768x574.png 768w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BackupBBI_lineshape_acetone.png 1076w\" sizes=\"(max-width: 624px) 100vw, 624px\" \/><\/a><\/p>\n<p>A 1D proton spectrum of Strychnine in CDCl3 : <a href=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BackupBBI_Strychnine.png\"><img decoding=\"async\" loading=\"lazy\" class=\"alignnone size-large wp-image-2686\" src=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BackupBBI_Strychnine-1024x763.png\" alt=\"\" width=\"624\" height=\"465\" srcset=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BackupBBI_Strychnine-1024x763.png 1024w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BackupBBI_Strychnine-300x223.png 300w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BackupBBI_Strychnine-768x572.png 768w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2022\/09\/BackupBBI_Strychnine.png 1074w\" sizes=\"(max-width: 624px) 100vw, 624px\" \/><\/a><\/p>\n<p>While we do everything we can to expedite the repair of the regular probe, I hope you will put this great probe to good use and keep obtaining the needed spectra for your research.<\/p>\n<p>The small inconvenience of tuning\/matching the probe by hand is a worthy price to pay to keep your work throughput at top level.<\/p>\n<p>Please approach either me or Adrienne, if you need further help.<\/p>\n<h2>NMR Facility Manager<\/h2>\n<h3>9.21.22<\/h3>\n<p>&nbsp;<\/p>\n<p>&nbsp;<\/p>\n<p>&nbsp;<\/p>\n","protected":false},"excerpt":{"rendered":"<p>Dear Users \u00a0\u00a0\u00a0\u00a0\u00a0 The regular probe with a faulty ATMA motor assembly is pulled out for repairs.\u00a0 Do not underestimate the probe that is placed in the magnet as a backup, because it is called Surrogate. This is a newly procured &#8220;gently used probe&#8221; in excellent condition and gives beautiful spectra as I show below. [&hellip;]<\/p>\n","protected":false},"author":19,"featured_media":0,"comment_status":"open","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":[],"categories":[11,21,9,7],"tags":[],"_links":{"self":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/2689"}],"collection":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/users\/19"}],"replies":[{"embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/comments?post=2689"}],"version-history":[{"count":1,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/2689\/revisions"}],"predecessor-version":[{"id":2690,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/2689\/revisions\/2690"}],"wp:attachment":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/media?parent=2689"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/categories?post=2689"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/tags?post=2689"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}