{"id":2901,"date":"2023-05-25T11:40:48","date_gmt":"2023-05-25T18:40:48","guid":{"rendered":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/?p=2901"},"modified":"2023-05-25T11:40:48","modified_gmt":"2023-05-25T18:40:48","slug":"appeal-neo500-let-us-keep-the-house-clean","status":"publish","type":"post","link":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/2023\/05\/appeal-neo500-let-us-keep-the-house-clean\/","title":{"rendered":"APPEAL &#8211; NEO500 :   LET US KEEP THE HOUSE CLEAN !"},"content":{"rendered":"<p>Dear NEO Users<\/p>\n<h3><strong>Appeal 1 : the problem of &#8220;Orphaned NMR Tubes&#8221;<\/strong><\/h3>\n<p>Please take a moment to behold the &#8216;status quo&#8217;\u00a0 of samples near the instrument that I recorded yesterday. <a href=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2023\/05\/IMG_6395.jpeg\"><img decoding=\"async\" loading=\"lazy\" class=\"alignnone size-large wp-image-2903\" src=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2023\/05\/IMG_6395-1024x768.jpeg\" alt=\"\" width=\"624\" height=\"468\" srcset=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2023\/05\/IMG_6395-1024x768.jpeg 1024w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2023\/05\/IMG_6395-300x225.jpeg 300w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2023\/05\/IMG_6395-768x576.jpeg 768w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2023\/05\/IMG_6395.jpeg 2048w\" sizes=\"(max-width: 624px) 100vw, 624px\" \/><\/a><\/p>\n<p><strong>Now, this is over and above all the holder positions of the sample Carousel being completely occupied during the time of the picture snapping. <\/strong><\/p>\n<p>With the ease of simply walking up to the instrument and loading your sample in the queue comes an inevitable cost.\u00a0 You can inadvertently clog up the pipeline pretty quickly.<\/p>\n<p><em>Given the fact that, even with\u00a0 &#8220;one sample at a time&#8221; operations on all the other instruments, users simply abandon their NMR sample tubes for Adrienne and I to deal with, I am not surprised that NEO500 is being afflicted with this pattern.<\/em><\/p>\n<p><strong>But we MUST mend our ways, and URGENTLY.\u00a0 We got quite a bit of flak from the recent EH&amp;S inspections about abandoned NMR tubes, with liquids of varying characters without any clue as to what those chemicals are ! We are on the watch list such that when the next inspection occurs, they don&#8217;t want to see this again. <\/strong><\/p>\n<h2>I am not a deciding authority, but if EH&amp;S concludes that the NMR facility is in constant violation on this front, whatever consequence that follows won&#8217;t be pleasant to any of you and your research goals.<\/h2>\n<p>You have been told about the following during NEO500 training and orientation :<\/p>\n<ul>\n<li><strong>Make note of when your sample&#8217;s acquisition will start from IconNMR&#8217;s interface<\/strong><\/li>\n<li><strong>Consider how much time your particular experiments will take to finish. Add a maximum of 5 minutes buffer for each unique sample as overhead (VT stability, Lock, Shim, etc.)<\/strong><\/li>\n<li><strong>Determine from the above, when your sample(s) will be done, approximately. <\/strong><\/li>\n<li>\n<h3><strong>Set a timer of your choice if needed, and stroll down to pick up your samples PROMPTLY.<br \/>\n<\/strong><\/h3>\n<\/li>\n<\/ul>\n<h2>ADDITIONAL SUPPORT :<\/h2>\n<ul>\n<li>You can always <a href=\"https:\/\/thermometer.chem.washington.edu\/cgi-bin\/iconqueue\">click on the following link<\/a> (even better, bookmark it) to check that your sample&#8217;s acquisition is done before taking the time to come down, in the midst of a busy day at the Chemistry bench.<\/li>\n<li>An automatic email feature that will send you both an alert after your sample is done and a PDF of the spectrum, is being tested and I hope to deploy this early next week.\u00a0 You will get a post on the same soon.<\/li>\n<\/ul>\n<h3><strong>Appeal 2 :\u00a0\u00a0 Need your help in clearing &#8216;Failed:&#8217;\u00a0 sample holder positions<\/strong><\/h3>\n<p>For many reasons, your acquisition run may be flagged as &#8216;<strong>Failed&#8217;<\/strong> by IconNMR.\u00a0\u00a0 When this happens,\u00a0 <strong>only <\/strong>the user who queued up that experiment AND the <strong>nmrsuperuser<\/strong> (i.e. me and Adrienne)\u00a0 will be able to delete that particular entry.<\/p>\n<p>Until that happens, no one can use that holder position.<\/p>\n<ul>\n<li><strong>When you come down to pick up your sample, look for those samples that &#8216;Failed&#8217; and the reason behind the same. <\/strong><\/li>\n<li><strong>If it&#8217;s an issue that requires time to address, such as your sample condition, please login as yourself and go to that holder position entry and delete it.<\/strong><\/li>\n<li><strong>If it is a momentary glitch that seemed to have disappeared (based on other successful runs after you), you can decide to resubmit that sample.<\/strong><\/li>\n<\/ul>\n<p>I show an example here. <a href=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2023\/05\/ICONNMR_failure_handling_ed.png\"><img decoding=\"async\" loading=\"lazy\" class=\"alignnone  wp-image-2902\" src=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2023\/05\/ICONNMR_failure_handling_ed-1024x195.png\" alt=\"\" width=\"703\" height=\"134\" srcset=\"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2023\/05\/ICONNMR_failure_handling_ed-1024x195.png 1024w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2023\/05\/ICONNMR_failure_handling_ed-300x57.png 300w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2023\/05\/ICONNMR_failure_handling_ed-768x147.png 768w, https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-content\/uploads\/2023\/05\/ICONNMR_failure_handling_ed.png 1776w\" sizes=\"(max-width: 703px) 100vw, 703px\" \/><\/a><\/p>\n<p>Either way, you can clear that particular holder so that the throughput is not affected. <strong>This becomes all the more important during those after office odd hours or weekends, when no one with the superuser privilege will be around to address it immediately. <\/strong><\/p>\n<p><strong>Thank you for your help with this. <\/strong><\/p>\n<h2>NMR Facility Manager<\/h2>\n<p>5\/25\/23<\/p>\n","protected":false},"excerpt":{"rendered":"<p>Dear NEO Users Appeal 1 : the problem of &#8220;Orphaned NMR Tubes&#8221; Please take a moment to behold the &#8216;status quo&#8217;\u00a0 of samples near the instrument that I recorded yesterday. Now, this is over and above all the holder positions of the sample Carousel being completely occupied during the time of the picture snapping. With [&hellip;]<\/p>\n","protected":false},"author":19,"featured_media":0,"comment_status":"open","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":[],"categories":[20,9,7],"tags":[],"_links":{"self":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/2901"}],"collection":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/users\/19"}],"replies":[{"embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/comments?post=2901"}],"version-history":[{"count":3,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/2901\/revisions"}],"predecessor-version":[{"id":2906,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/2901\/revisions\/2906"}],"wp:attachment":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/media?parent=2901"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/categories?post=2901"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/tags?post=2901"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}