Hello All<\/p>\n
Following an unfortunate incident of a user dropping the sample tube into the magnet bore without a spinner,\u00a0 it turned out that the sample tube broke inside the new iProbe probehead.\u00a0 Being a mint condition probe, which also belongs to the latest generation, it will need careful handling in assessing the extent of damage and the remedial measures that ought to be planned.<\/p>\n
To minimize the instrument downtime I have placed the TXO-1H{19F,13C}-Z gradient probe as the surrogate.\u00a0 <\/strong><\/p>\n This is a familiar probe to all of you.\u00a0 What more, this will replicate the outgoing iProbe’s capabilities of : (1) 19F observe with 1H decoupling and (2) running true 19F-1H double resonance experiments.<\/p>\n You can use Topshim as usual to get the good resolution and lineshape without drudgery. But, remember, there is NO ATMA !<\/strong>\u00a0 You must tune\/match the probe by hand.<\/p>\n Of course, we will take all the necessary measures without delay to revive the iProbe to its original glory and put it in the magnet, as soon as possible.<\/strong><\/p>\n 6\/9\/2023<\/p>\n <\/p>\n","protected":false},"excerpt":{"rendered":" Hello All Following an unfortunate incident of a user dropping the sample tube into the magnet bore without a spinner,\u00a0 it turned out that the sample tube broke inside the new iProbe probehead.\u00a0 Being a mint condition probe, which also belongs to the latest generation, it will need careful handling in assessing the extent of […]<\/p>\n","protected":false},"author":19,"featured_media":0,"comment_status":"open","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":[],"categories":[11,21,9],"tags":[],"_links":{"self":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/2924"}],"collection":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/users\/19"}],"replies":[{"embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/comments?post=2924"}],"version-history":[{"count":1,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/2924\/revisions"}],"predecessor-version":[{"id":2925,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/posts\/2924\/revisions\/2925"}],"wp:attachment":[{"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/media?parent=2924"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/categories?post=2924"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/depts.washington.edu\/chemwp\/chemwpnmr\/wp-json\/wp\/v2\/tags?post=2924"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}TOPSHIM is there !<\/strong><\/h2>\n
As always, thank you for your cooperation.\u00a0 The instrument will be released for reservation in the next ten minutes or so.<\/strong><\/h3>\n
NMR Facility Manager<\/h2>\n