GEMSEC

Using Nanoscience Instrumentation for

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Nanotechnology Undergraduate Education (NUE)

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NUE – UNIQUE – LAB

Workshop: Nanoscience on the Tip

PDF DOWNLOAD OF SPM WORKSHOP Material 2007 & 2008

        

Nanotechnology Undergraduate Education (NUE)

NUE UNIQUE SPM WORKSHOP: Nanoscience on the Tip

 

    

Location: University of Washington, Seattle, WA

 

Workshop costs are covered by NUE UNIQUE, a NSF sponsored undergraduate program. Travel and accommodation for MRSEC students outside the UW are sponsored by GEMSEC.

 

Application is closed for 2008.

 

Objective and Background

The objective of this intensive SPM workshop is to provide a truly hands-on experience (3-4 students per instruments) in a classroom laboratory setting involving a variety of SPM techniques applied to nanoscience and nanotechnology aspects related to chemistry, physics and biology.

Since the invention of the scanning tunneling microscope (STM) in 1981 by Gerd Binnig and Heinrich Rohrer (Nobel Prize in Physics 1986) scanning probe microscopy (SPM) techniques have dazzled scientist and engineers in nearly every field from natural sciences to liberal arts, and nucleated the new discipline of Nanoscience and Nanotechnology. The birth of such a highly interdisciplinary field is an attest to the changing times in a world that moves from educating specialists to generalists. The true power of SPM techniques, which assisted in removing boundaries between disciplines, lays in its simplicity to provide access to nanoworld in terms of visualization and manipulation. Hence, it is only perceivable that SPM offers outstanding educational tools for schools.

 

Synopsis and List of Laboratory Units

Students will gain hands-on experience involving a wide variety of nanotechnology/nanoscience applications, using some of the most versatile nano-tools based on Scanning Probe Microscopy (SPM). With an intensive one-week schedule and a low student to instrument and student to TA ratio of 4:1, deep and lasting learning will occur. The intense 40 hours one-week workshop will provide students with the opportunity to apply their theoretical knowledge from prior lecture courses.

 

Laboratory Units (developed for 2007 and 2008 Workshop)

 

Lab Unit I:      Scanning Force Microscopy and Dip-Pen Nanolithography

The student will become familiar with contact mode Scanning Force Microscopy (SFM) as an imaging technique, and be introduced with Dip-Pen Nanolithography (DPN).

Lab Unit IB:   Introduction to Scanning Force Microscopy

The student will become familiar with contact mode Scanning Force Microscopy (SFM) as an imaging technique and as ultra-sensitive force sensor.

Lab Unit II:     AC-Mode imaging and Electrostatic Force Microscopy

This lab unit introduces Electrostatic Force Microscopy to characterize the electrical properties of a blended conjugated polymer film by studying the changes in tip oscillation due to electrostatic force gradients between the tip and the sample.

Lab Unit IIB: Binding  Kinetics of Proteins

In his lab unit students are characterizing protein-material using intermittent non-contact (NC) scanning force microscopy (SFM) in both fluid medium and in air to quantify surface adsorption. The material analyzed are graphite adsorbed  blood clotting proteins, fibrinogen (Fb), to mimic a bio-response to prosthetic heart valve devices.

Lab Unit III:    Force Spectroscopy Analysis

This lab unit introduces a scanning force microscopy (SFM) based force displacement (FD) technique, FD analysis, to study local adhesion, elastic properties, and force interactions between materials.

Lab Unit IV:   Force Modulation Microscopy

This lab unit introduces a scanning force microscopy (SFM) based mechanical (sinusoidal) perturbation method referred to as force modulation microscopy, to explore thermomechanical properties in polymers around the glass transition.

Lab Unit V:     Scanning Tunneling Microscopy

This lab unit introduces scanning tunneling microscopy (STM) technique, used to obtain real space atomic resolution images of conductive surfaces. The tunneling spectroscopy mode of STM is employed to examine local density of state (LDOS) of the surface.

 

List Lab Units under Constructions:

Lab Unit:          Nanocomposites

In this unit, students will be introduced to nanocomposites and the challenges involved in establishing material phase contrast with AFM. AFM and transmission electron microscopy will be employed to analyze materials. Educational outcomes: Familiarize students with nanocomposite materials and their potential in generating unique properties, such as reversed selectivity in membranes.

Lab Unit:          Molecular Mobility and Organic Electronics

Students will be introduced to organic electronics and exposed to the challenges involved in non-linear optical organic polymer materials used for photonic applications. The aim is to achieve effective device performance by utilizing submolecular relaxations.  Educational outcomes: The students will learn about molecular mobility in polymers, the concept of the widely used superposition principle, and an AFM based method.

 

Instructors

Prof. David Ginger (Chemistry) research focuses on the creation and study of nanostructured materials with unique optoelectronic and photonic properties.  His group has pioneered novel scanning probe microscopy and lithography methods to further our understanding of nanostructured organic solar cells.  His group is also developing bioinspired assembly strategies for controlling near-field electromagnetic coupling between fluorophores and plasmon resonant nanoparticles. Ginger is also known for his work in the development of semiconductor nanocrystals for photovoltaics and LEDs, and as a pioneer of Dip-Pen Nanolithography methods for biomolecules.  In recognition of his research and education efforts he has been named a Research Corporation Cottrell Scholar.

Prof. René M Overney (Chem. Eng.) is known for his pioneering work in nanorheology and transport properties. His group has developed various SPM nano-characterization methods particularly applicable to polymer science and related technologies. The research of his group ranges from mesoscale material aspects in photonics, optoelectronics, electronic storage media, PEM fuel cell, tribology to human implant technology. Overney coauthored of one of the early textbooks in Nanoscience (Nanoscience, World Scientific 1998), and is teaching on the undergraduate and graduate level nanoscience related courses since 1996.

Prof. Mehmet Sarikaya (Mat. Sci.) is known for his pioneering efforts and ideas in Molecular Biomimetics. By merging recent advances in molecular biology and genetics with state-of-the-art engineering and nanocharacterization from the physical sciences, his and his collaborators’ goal is to shift the biomimetic materials science paradigm from imitating Nature to designing materials to perform artificial nanofunctions. It is the intent to combine Nature’s proven molecular tools, such as proteins, with synthetic nanoscale constructs to make molecular biomimetics a full-fledged methodology. To this end, at the Genetically Engineered Materials Science and Engineering Center, an NSF-MRSEC, Sarikaya is directing a multidisciplinary team with diverse expertise to genetically select inorganic-binding short polypeptides, tailoring them via molecular manipulation and bioinformatics to make heterofunctional molecular constructs and using them as synthesizers, assemblers, and molecular erectors in materials science and medicine.

 

Eligibility Requirement

To be eligible for the program you must be:

 

1. UG student in the second year enrolled at a 4 year higher educational institution or senior student in a 2 year higher educational institution (e.g., Community College),

2. Majoring in engineering, materials science, chemistry, or physics,

3. Available to participate throughout the entire SPM Workshop.

Successful applicants are responsible for travel and adequate insurance.