UW CHEMISTRY NMR

Announcments & Equipment Logs

March, 2023

UPDATE ! GG500 – SHIMMING OK

Dear Users The Warning message noted today related to preamplifier and the failure of Topshim were related and the root cause is identified and eliminated. The system is shimming as before and everything is back to normal. NMR Facility Manager 3/28/23

Posted in Hardware, Spectrometer | No Comments »

REMINDER ! PLEASE RESERVE YOUR NMR TIME FOR GG500 AND 300 INSTRUMENTS !

Dear Users While we are very happy to see that you are all getting comfortable with the truely ‘walk-on’ nature of running NMR with our new NEO500 system,  unfortunately,  this process cannot yet be replicated on the other instruments. Until we get a fully automated setup  with multiple sample handling on the other instruments, YOU […]

Posted in Spectrometer, Usage | No Comments »

UPDATE ! NEO500 – WILL ACCEPT SAMPLES FROM 3 PM

Dear Users The hardware replacement is complete and the tests have passed.  You can start queuing samples from 3 PM. NMR Facility Manager 3/16/2023

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UPDATE ON NEO500 – SYSTEM WILL GET TO MAINTENANCE MODE IMMEDIATELY

Hello All The hardware parts reached earlier than exepcted, and the system is not shimming at all with the current configuration. It makes sense, therefore, to swap the hardware without any further delay and test it. As an upside, if everything goes well,  the instrument will be released much earlier than expected. Please wait for […]

Posted in Hardware, Spectrometer | No Comments »

ALERT ! NEO500 – SYSTEM WILL BE DOWN BRIEFLY FROM 1.30 PM FOR HARDWARE WORK

Hello Users The remedial circuit boards that should resolve the intermittent Shim failure, will be installed and tested in the system starting from 2 PM and a bit of preparation is needed before that. Please do NOT queue any samples after 1 PM today. Any halted runs between 1 PM and the instrument down time […]

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NEO500 : IMPORTANT CLARIFICATION ABOUT TUBE LENGTHS

Dear Users While you were trained on the new NEO500 system, you were told that it is OK to use the J-Young type tubes even with this fully automated system.   This is definitely true, but certainly there is a caveat to that statement. Please look at the picture below.   The ‘dotted line’ is roughly the […]

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ALERT ! NEO500 – SHIM QUALITY ISSUES

Dear Users Many of you might have noticed that the lineshape and resolution you got for many of your samples in the past several days are not what you expected, that too from a mint condition instrument such as NEO500. We are aware of this and have been applying remedies to resolve this transparently.  I […]

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UPDATE ON AV300 : SYSTEM HAS UPGRADED VT CONTROL NOW !

Dear Users Thanks to a low temperature chiller that we repurposed from the recently decommissioned AV500 console,  the AV300 system now has much better temperature stability and also the capability to lower your sample temperature close to 0 deg. C, if you wish to. Temperature stability is quite important, when it comes to Lock and […]

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CLARIFICATION ABOUT MY ACCESSIBILITY, AVAILABILITY….AND AN APPEAL….

Dear fellow NMR enthusiasts and valuable users : Ever since the day I have been honored with managing this amazing NMR facility and help with the clientele, it has been a fact that the NMR Manager is a highly delocalized particle, to borrow a phrase from the world of Quantum Mechanics. The geographical locations that […]

Posted in NMR Facility Usage, Uncategorized | No Comments »

UPDATE ! NEO500 – BUDGET NUMBERS ACTIVELY CHECKED FOR ACCURACY

Dear Users Thank you for paying attention to the mandatory entry of your valid budget number when you queue up an experiment on NEO500.   To help you with this process, a software plugin of sorts is now activated. When you enter a budget string that is incorrect, you will be alerted with Red font as […]

Posted in NMR Applications | No Comments »

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