UW CHEMISTRY NMR

Announcments & Equipment Logs

August, 2021

NOTE : RETURN OF NMR RESERVATION TO USUAL SCHEDULE

Dear Users Although what follows might sound intutive for many of you who have been following the University’s COVID related guidelines of late,  I will still mention this formally, in line with the expected full strength in-person opening of UW for the fall quarter. The mandatory 10 minute ‘book ending’ gap before and after a […]

Posted in NMR Facility Usage | No Comments »

UPDATE : AV500 – SHIM SYSTEM TAMED – MOSTLY

Dear Users I mentioned last week that a couple of hardware related issues need addressing and this is an update about the first and foremost of them :  getting consistent results from Topshim method of shimming for all Lock Solvents.   The root cause for the sporadic failure of Topshim, especially for weak lock signals […]

Posted in Hardware, NMR Applications, Spectrometer, Usage | No Comments »

UPDATE : FTP DATA SERVER PHOENIX IS BACK ONLINE

Should be able to access downlodable data, especially from GG500 without issues now. Please let me know otherwise. NMR Facility Manager 8/15/21

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ALERT ! PHOENIX DOWN TEMPORARILY

The FTP system hasn’t come up after the power interruption on Friday evening and we are looking into it. Will provide an update once it is online. NMR Facility Manager 8/15/21

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UPDATE ! : ALL NMR SYSTEMS ARE REVIVED BACK

Dear Users Systems are ready for use.   As to the Power being pulled at 3.30 pm yesterday i.e. earlier than announced,  everyone was taken by surprise including the building co-ordinators.     Indeed it was unexpected but we couldn’t do much about it ! Good Day NMR Facility Manager 8/14/2021

Posted in Spectrometer, Usage | No Comments »

ALERT ! AV500 – HEADS UP ON THE SHIM RELIABILITY

Dear Users Some of you might have noticed the following but may have chosen to ignore this, since it didn’t affect your 1H spectra much.    The current TXO probe is not providing good 2H based shimming results and it needs some close attention. Currently, the instrument can fail to give you good lineshape or Topshim […]

Posted in Hardware, Spectrometer | No Comments »

UPDATE : AV300 – SYSTEM BACK TO NORMAL

Dear Users I have checked that the ATMA operation is now as expected.   Please let me know if you notice anything otherwise. If any of you use a lock solvent that is typically out of the ordinary and if you face an ATMA problem, please contact me immediately.   It will be a great help. NMR […]

Posted in Hardware, Spectrometer | No Comments »

ALERT ! AV300 – DOWN DUE TO PROBE ISSUE

Dear Users The ATMA function is not giving the expected result and it is being looked into.  The instrument will be down until further notice. Please look for an update from me on this later today. NMR Facility Manager 8/13/21

Posted in Hardware, Spectrometer | No Comments »

HEADS UP ! NMR FACILITY WILL BE POWERED DOWN FOR PLANNED ELECTRICAL MAINTENANCE

Dear Users         All the NMR instruments in the facility will be powered down on or after 4 pm today i.e. Friday the 13th,  in preparation for a building wide power shut down by UW Facilities and Services for planned Electrical Maintenance The instrument will be revived tomorrow morning i.e. Saturday, the 14th.   I am […]

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UPDATE ! AV300 – NON-UDRIVE STORAGE RESTORED

Dear Users A new local storage system is put in place, to replace the failed hard drive that caused a problem a few days ago, if you recall. As a result,  so-called ‘external users’ or ‘sponsored Netid users’ can use AV300 as before and download their data from the FTP server, as before. If you […]

Posted in Datasets, Host Computer, Operating System | No Comments »

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