UW CHEMISTRY NMR
Announcments & Equipment Logs
ALERT ! NEO500 – ICONNMR AUTOMATION RESTARTED
The Prodigy cryoprobe is ready to accept samples. Please queue up your runs as usual. If you have questions, please reach out. Thank you for your patience. NMR Facility Manager 8.25.25
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ALERT ! NEO500 – PRODIGY PROBE IN SERVICE MODE TILL MONDAY
Dear Users We need to warm up the cryoprobe and do some additional preventive maintenance routines on the reborn Prodigy probe. This will ensure that the Probe specifications return to the promised values by the manufacturer (they are just short of the target) the expensive hardware components that were replaced are functioning upto snuff within […]
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UPDATE ! NEO500 – PRODIGY PROBE IS READY FOR USE
Dear Users You can start queueing up samples as before via IconNMR interface with the Prodigy Probe. Those of you who haven’t used the instrument before, please contact me first. Please remember and honor the important points I announced in the prior Post, in using the Prodigy system. Thank you for your patience, all along. […]
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UPDATE ! NEO500 – PRODIGY HAS RISEN FROM ASHES – PLEASE READ
Dear Users After the long and inevitable wait, the Prodigy probe has been resurrected (with a stiff price tag) and returned to us by the manufacturer. We also had to replace failing components in associated hardware that runs the probe. The probe is being tested now. We will hopefully deploy the instrument for regular use […]
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UPDATE ! GG500 – AUTOMATION QUEUE RESUMED
Can submit samples as usual. NMR Facility Manager 8.6.25
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ALERT ! GG500 – AUTOMATION QUEUE WILL RESUME AFTER HELIUM FILL
Automation queue will stop during the Helium fill from 10.30 am to 12 noon. The queued experiments will resume after the fill is completed. Always check the instrument reservation calendar, before heading down to the instrument for queuing up samples. NMR Facility Manager 8.6.25
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UPDATE ! GG500 – AUTOMATION QUEUE RESUMED
You can start submitting samples. Sample inject/eject issue is addressed. NMR Facility Manager 7.30.25
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ALERT ! GG500 – SYSTEM DOWN DUE TO SAMPLE HANDLING ISSUE
The sample eject/inject problem, led to the crash of the automation queue this morning. The system will be down until further notice to identify and remedy the issue. I will post an update once the queue is resumed. NMR Facility Manager 7.30.2025
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UPDATE – NEO500 – PROBE IS FULLY FUNCTIONAL WITH TOPSHIM
Dear Users The probe is optimized for different lock solvents that should make shimming with Topshim quick and easy. I have created individual shim files that are the optimal starting points for the most often used lock solvents. The files are named as below : txo.water (for aqueous samples, including those in D2O) txo.acteone txo.cdcl3 txo.c6d6 txo.dmso […]
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UPDATE ! NEO500 – PROBE CHANGED TO TXO-19F{1H,13C} – PLEASE NOTE
Dear Users The previous TBI probe had to be removed for a service operation, and I have placed the TXO-19F PROBE for the present as an alternative. Please note the following : Nuclei : 19F, 1H and 13C You can run 1H decoupled 19F experiments To switch between 19F and 13C, a cable swap is needed […]
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