UW CHEMISTRY NMR

Announcments & Equipment Logs

June, 2024

GG500 – PLANNED MAINTENANCE , Jul. 1 Mon – IMPACT

For better part of the day on Jul. 1, Monday, the system will be down for hardware maintenance.  The automation queue will be stopped early in the morning that day.  Do not plan to queue any experiments from 8 AM. The Automation queue should resume from 5 PM latest, that day, but for unexpected contingencies. […]

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UPDATE : GG500 – SWITCH TO MANUAL MODE LATER TODAY

Due to the HVAC radiator maintenance and asbestos mitigation of the NMR lab yesterday,  the automation queue could not be continued from 4.30 pm. The system will attempt to complete the pending queue before it is switched to Topspin direct login. NMR Facility 6/18/24

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PLEASE NOTE : UW FACILITIES WORK IN NMR ROOM

Please bear with us for not able to bring this update earlier.  Facilities and Services is taking care of a long overdue Radiator Work and residual asbestos mitigation on some tiles in Room:33 (NEO500) and Rm.37 (GG500 and 300 NMRs), today and tomorrow. They have scheduled it to have minimal impact to the operation to […]

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UPDATE ! GG500 – READY FOR AUTOMATION RUN – PLEASE QUEUE UP SAMPLES

Few reminders : You can download your data via the FTP server link:  phoenix.chem.washington.edu/GG500. You can set the temperature you desire, from the Automation Window itself.   The software will check the target temperature before starting the run A cumulative maximum of 60 minutes per sample holder position will be treated as a ‘walk-on’ run and […]

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NOTE ! GG500 – WILL ENTER ICONNMR AUTOMATION TOMORROW – FRI 14TH

The Topspin ICONNMR interface will be deployed starting noon tomorrow i.e. Friday, the 14th.   It is very similar to the NEO500 interface.  Here are points that are unique to GG500. Access : The system will be in Full IconNMR Automation mode from Friday morning 10 AM of a given week and continue till 10 AM […]

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UPDATE : NEO500 – READY FOR USE

The queue is started.  Please line up samples. NMR Facility

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UPDATE : PHOENIX FTP SERVER ONLINE

All files are downloadable.  Please let us know, otherwise. NMR Facility (contact:  amr0311@uw.edu; rajanp@uw.edu)

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UPDATE : ALL SYSTEMS (EXCEPT NEO500) READY FOR USE

As mentioned previously,  NEO500 and Prodigy probe will be ready to accept samples in Automation queue by noon tomorrow i.e. Tuesday, the 11th. All other systems are ready for immediate use. NMR Facility (contact : amr0311@uw.edu; rajanp@uw.edu)

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ALERT ! BAGLEY ELECTRICAL SHUTDOWN ON MONDAY – IMPACTS

Approximately by evening of Sunday, 9th June,  all NMR instruments will be powered down, in anticipation of an early morning electrical disruption next day i.e. Monday. All instruments, except the NEO500 with Prodigy Cryoprobe should be revived by noon on Monday, the latest. NEO500 will be released for regular use by Tuesday, 11th, morning. Please […]

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GG500 : SYSTEM READY FOR USE – SAMPLE TUBE BREAKAGE FIXED

Based on what we observed,  a sample tube broke while a user loaded the sample with spinner into the Carousel.  This triggered an error condition of the Sample Robot. PLEASE PAY ATTENTION : With the Automation Hardware in place, we have reduced the physical human interaction with NMR machine to just a single step :  […]

Posted in Hardware, Spectrometer | No Comments »

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