UW CHEMISTRY NMR

Announcments & Equipment Logs

Hardware

GG500 – PLANNED MAINTENANCE , Jul. 1 Mon – IMPACT

For better part of the day on Jul. 1, Monday, the system will be down for hardware maintenance.  The automation queue will be stopped early in the morning that day.  Do not plan to queue any experiments from 8 AM. The Automation queue should resume from 5 PM latest, that day, but for unexpected contingencies. […]

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NOTE ! GG500 – WILL ENTER ICONNMR AUTOMATION TOMORROW – FRI 14TH

The Topspin ICONNMR interface will be deployed starting noon tomorrow i.e. Friday, the 14th.   It is very similar to the NEO500 interface.  Here are points that are unique to GG500. Access : The system will be in Full IconNMR Automation mode from Friday morning 10 AM of a given week and continue till 10 AM […]

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GG500 : SYSTEM READY FOR USE – SAMPLE TUBE BREAKAGE FIXED

Based on what we observed,  a sample tube broke while a user loaded the sample with spinner into the Carousel.  This triggered an error condition of the Sample Robot. PLEASE PAY ATTENTION : With the Automation Hardware in place, we have reduced the physical human interaction with NMR machine to just a single step :  […]

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ALERT : GG500 – SAMPLE CHANGER ERROR

We are looking into the sample changer issue and will post an update as soon as it is resolved. NMR Services Manager 6/5/2024

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UPDATE – NEO500 : ATMA issue resolved

Check the quality of your data if it was processed by the system before 3 pm today.  If it is not satisfactory,  please resubmit it. ATMA was non-functional until 2.45 pm.  But the default tune/match might have been good for some of the samples. If that’s the case, the data collected should be OK. NMR […]

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Update GG500 – Autosampler status

The work installing the new Sample Case Plus with 60 sample holders is complete. The GG500 is currently on the reservation system as regular operation. However, with the new Sample Case Plus, the protocol for inserting samples has changed! If you have not been trained to use the GG500 with the new Sample Case Plus, […]

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NEWS ! GG500 – WE ARE ADDING AN AUTOMATED SAMPLE CHANGER

Dear Users In the span of next week, you will see a ‘twin incarnation’ of the automatic sample handler that you see on NEO500 called SampleCase, appearing alongside the GG500 system and tested.  We will give a headsup as to when this will happen with as much lead time as possible, but the installation process […]

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UPDATE ! GG500 – OLD DATASETS RESTORED

Dear Users We have restored the raw datasets from the failed computer that went down around 2nd Apr., into the new system.  All the active users in our database should be able to access their old datasets via the phoenix server.    If something is missing, please contact us and let us know. I would repeat […]

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UPDATE ! GG500 – READY FOR RESERVATION AND USE

Dear NMR community GG500 instrument is ready for use again.   Please note the following : Topshim is working nominally.  For deuterium based lock solvents, which means the majority of them,  the shimming happens along the Z-axis only (known fact and a feature of the spectrometer hardware). You can start Topshim after loading the default starting […]

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UPDATE ! GG500 – ALMOST READY – PLEASE SEE BELOW

Dear Users First of, thank you for your patience. The computer driving the instrument needed a complete replacement, which is an elaborate operation involving properly restoring data and configuration files and make sure that the spectrometer is being driven correctly by this new PC.  These operations are largely done. Quite independent of this, recently we […]

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