UW CHEMISTRY NMR
Announcments & Equipment Logs
Software
IMPORTANT NOTE ! – FACILITY SHUT DOWN DUE TO PLANNED POWER OUTAGE
All of you must have seen the confirmation mail from Brian Holm that on Jan 25th, Saturday and Feb. 1st, Saturday, Bagley Hall will be without power for a couple of hours. In this connection, the NMR Facility will be shut down by the evening of Jan. 24th, 4.00 pm and Feb 1st, 4.00 pm. The systems […]
Posted in Hardware, Software, Spectrometer, Usage | No Comments »
AV300 – UPDATE : HANGING PROCESS CLEARED
The login crash is resolved and users should be able to use Topspin without issues. Please post a feedback if you find otherwise.
Posted in Software, Spectrometer, Usage | No Comments »
AV500 : 31P MACRO FUNCTIONAL
Users who are used to typing ‘phosph’ and load the standard 31P {1H} decoupled parameter set are invited to use the same once again. The glitch that was preventing the pulse widths and power levels being loaded is remedied. Any observation you make to the contrary will be much appreciated as a log post.
Posted in Software, Spectrometer, Usage | No Comments »
ALERT ! AV500 UPDATE : UWNetid FUNCTIONAL – AGAIN
Users are requested to note that they can user their UWNetid login as before to operate the NMR spectrometer. A new operating system platform has been installed to address the vexing problem of Netid login failure. This transition should provide trouble free UWNetid login as well as a smooth execution of all the Topspin automation […]
Posted in Hardware, Software, Spectrometer, Usage | No Comments »
AV500 UPDATE : PROPER SETUP OF EXPERIMENTS
Following the reconfiguration of the Lock system, users need to observe the following procedure to get correct results. If you are copying an old data set to start a new run, please run the edasp command. You will see a graphical window similar to the following : Click on the Save button to exit. Your […]
Posted in Software, Spectrometer, Usage | No Comments »
AV500 : LOCK UPDATE
Users had noted that the intermittent lock issue was back again. A careful scrutiny was made and a needed configuration change was made to solve this problem. The system should lock on all solvents without any error now. If it is otherwise, please do note the same in the Log Book along with any other […]
Posted in Hardware, Software, Spectrometer | No Comments »
AV500 : AUTOMATION SCRIPTS COMPILATION ISSUES
There is a software glitch that is preventing the proper compilation of several automation scripts, including the commonly used ones such as ‘iexpno’ or ‘multizg_vd’. We are working on this and I will post an update once this issue is resolved.
Posted in Software, Spectrometer | No Comments »
AV800 : UPDATE – SYSTEM STILL UNSTABLE
Thorough investigations thus far indicate two possible points of instability in the system that leads to sporadic and unpredictable failure of the spectrometer. Since a troubleshoot of this nature entails long periods of test runs and observations, the system is not ready to collect useful data yet. We will keep users posted as to any […]
Posted in Hardware, Software, Spectrometer | No Comments »
AV500 UPDATE : Screen Freeze Resolved
Users can drag and drop the datasets as before, if they prefer that method. The spectrum screen will not freeze with this operation. Nevertheless, the Right Click has a context menu that has more items that are useful, other than opening the dataset.
Posted in Software, Spectrometer, Usage | No Comments »
AV500 Note : screen freeze when you try do drag and drop a dataset
A software patch needs to be applied to remove the issue of screen freezing when you drag and drop an existing data set from the File Browser onto the Topspin spectrum window. To circumvent this currently, please Right Click on the dataset and choose the ‘Open’ or ‘Open in New Window’ from the menu that […]
Posted in Software, Spectrometer | No Comments »