UW CHEMISTRY NMR

Announcments & Equipment Logs

Usage

ALERT ! NEO500 – ICONNMR AUTOMATION RESTARTED

The Prodigy cryoprobe is ready to accept samples.  Please queue up your runs as usual.  If you have questions, please reach out. Thank you for your patience. NMR Facility Manager 8.25.25

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ALERT ! NEO500 – PRODIGY PROBE IN SERVICE MODE TILL MONDAY

Dear Users We need to warm up the cryoprobe and do some additional preventive maintenance routines on the reborn Prodigy probe.  This will ensure that the Probe specifications return to the promised values by the manufacturer (they are just short of the target) the expensive hardware components that were replaced are functioning upto snuff within […]

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UPDATE ! NEO500 – PRODIGY PROBE IS READY FOR USE

Dear Users You can start queueing up samples as before via IconNMR interface with the Prodigy Probe. Those of you who haven’t used the instrument before, please contact me first. Please remember and honor the important points I announced in the prior Post, in using the Prodigy system.  Thank you for your patience, all along. […]

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UPDATE ! NEO500 – PRODIGY HAS RISEN FROM ASHES – PLEASE READ

Dear Users After the long and inevitable wait, the Prodigy probe has been resurrected (with a stiff price tag) and returned to us by the manufacturer.  We also had to replace failing components in associated hardware that runs the probe.  The probe is being tested now.  We will hopefully deploy the instrument for regular use […]

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UPDATE ! GG500 – AUTOMATION QUEUE RESUMED

Can submit samples as usual. NMR Facility Manager 8.6.25

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ALERT ! GG500 – AUTOMATION QUEUE WILL RESUME AFTER HELIUM FILL

Automation queue will stop during the Helium fill from 10.30 am to 12 noon. The queued experiments will resume after the fill is completed. Always check the instrument reservation calendar, before heading down to the instrument for queuing up samples. NMR Facility Manager 8.6.25

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UPDATE ! GG500 – AUTOMATION QUEUE RESUMED

You can start submitting samples.  Sample inject/eject issue is addressed. NMR Facility Manager 7.30.25

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UPDATE – NEO500 – PROBE IS FULLY FUNCTIONAL WITH TOPSHIM

Dear Users The probe is optimized for different lock solvents that should make shimming with Topshim quick and easy. I have created individual shim files that are the optimal starting points for the most often used lock solvents. The files are named as below : txo.water (for aqueous samples, including those in D2O) txo.acteone txo.cdcl3 txo.c6d6 txo.dmso […]

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GG500 : ALL GOOD – AUTOMATION QUEUE IS UP AND RUNNING

Frozen interface is fixed.  The original queue is resumed.    You can submit samples as usual. NMR Facility Manager 7.25.2025

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ALERT ! NEO500 – TOPSHIM MALFUNCTIONING

Topshim is not performing optimization although the software goes through the motions.  We are looking into it and will give an update as and when feasible. The shim system  is alive i.e. you can shim the sample by hand if all else fails. We will keep you updated. NMR Facility 7.11.25

Posted in Software, Spectrometer, Usage | No Comments »

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