UW CHEMISTRY NMR

Announcments & Equipment Logs

Spectrometer

DRX499 – INSTRUMENT DOWN DUE TO USER ERROR

A user has managed (again) to drop a sample tube without a spinner into the magnet bore.  Currently we don’t know the extent of damage this has caused but we are investigating. An update will be posted once the instrument is revived back to usability.

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AV700 UPDATE : SYSTEM IS REVIVED

The workaround is functional and the spectrometer is working again.  The probe change to solids will be completed today, as planned.

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AV700 ALERT : SYSTEM DOWN DUE TO PNEUMATICS PROBLEM

The proposed probe change is postponed to tomorrow since the console has a damaged filter system.  A workaround is being tried and if the console can be revived immediately, then we will be on track with the original schedule.  An update will be posted in due course.

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AV700 : PROBE CHANGE ALERT

The solutions HCN probe will give way to the solids MAS probe come Monday, the 6th of May ’13.  The spectrometer will serve the solids work needs for about four weeks from this date.

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AV500 – POSSIBLE VT ISSUE

Users have mentioned that they are not able to bring the VT set point below approx. 285 K. We are looking into this and an update with more information and planned remedy will be posted here. Stay tuned…

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AV500 UPDATE : Screen Freeze Resolved

Users can drag and drop the datasets as before, if they prefer that method.  The spectrum screen will not freeze with this operation.  Nevertheless, the Right Click has a context menu that has more items that are useful, other than opening the dataset.

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AV500 Note : screen freeze when you try do drag and drop a dataset

A software patch needs to be applied to remove the issue of screen freezing when you drag and drop an existing data set from the File Browser onto the Topspin spectrum window.   To circumvent this currently,  please Right Click on the dataset and choose the ‘Open’ or ‘Open in New Window’  from the menu that […]

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AV500 UPDATE : DATA ACCESS RESTORED….

The intermittent data access issue is resolved.  Users are requested to note that, there is a fall back available in situations when data is not seen from Phoenix.  You can directly upload the data files to the UW cloud storage or any other suitable third party storage via the web browser. Although this is not […]

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AV800 – IMPORTANT INFORMATION

Users of 800 spectrometer are reminded that the power outage on April 13 resulted in issues with the cryopanel. Those issues have been resolved. However, other issues remain, rendering the system unusable. Every effort is being put in, to revive the spectrometer as quickly as possible.   Please look for further updates on this issue.  Contact Rajan […]

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ALERT ! AV500 UPDATE – SYSTEM BACK TO NORMAL

The auto locking issue has been resolved. Users can start booking time with immediate effect. Please contact Facility staff if you need any assistance.  Thank you very much for your kind patience all along.

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