UW CHEMISTRY NMR

Announcments & Equipment Logs

Spectrometer

ALERT : NMR PRINTER OUT OF ORDER

An irrecoverable hardware problem has been found with NMR room printer.  Until we procure an alternate solution, users are requested to do their printing in their lab/office printers.  You can create printable  .jpg or .pdf images of the spectra from the NMRJuicer computer and send the same to your email account OR store in a […]

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AV500 ALERT : SYSTEM IS OPERATIONAL AGAIN

Users can start reserving time.  Thank you very much for your kind understanding and patience all these days, especially with multiple instruments being down.  Please do not hesitate to contact one of the facility staff if you need any assistance.

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AV301 UPDATE : 1H {13C} PROBE WITHOUT VT VARIATION

This old double resonance probe cannot do VT variation.  The lineshape as it exists is usable for the routine runs but needs further optimization.  Since this probe will be treated only as a temporary resource, we are releasing the instrument as it is, to reduce the deficit of dysfunctional instruments to one i.e. AV500.   PLEASE […]

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UPDATE : NMR SYSTEM UP AFTER POWER OUTAGE

Users can start use of the instruments as usual.  Please let us keep informed if anything unusual is noticed, since problems lurking generally come out after a power cycle.

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REMINDER : NMR FACILITY DOWN DURING PLANNED POWER OUTAGE

There will be a planned power outage in Bagley Hall this Saturday, the 18th, which will affect the NMR facility instruments as well.  The instruments will therefore be turned off by 4.00 pm, Friday the 17th and restored after the electrical maintenance is completed.

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AV500 : UPDATE – DAMAGED HARDWARE

An issue has been identified with the RT shim stack and this makes the instrument unusable currently.  Since repair of this part is not feasible in house, we have to wait for a replacement of the same.   Users will be updated on that front when more information is available.

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ALERT ! AV500 DOWN…

Hardware malfunction is being investigated.  The instrument will be down possibly until tomorrow.  Further updates will be posted here.    

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AV800 : UPDATE – SYSTEM STILL UNSTABLE

Thorough investigations thus far indicate two possible points of instability in the system that leads to sporadic and unpredictable failure of the spectrometer. Since a troubleshoot of this nature entails long periods of test runs and observations, the system is not ready to collect useful data yet.   We will keep users posted as to any […]

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ALERT AV301 : PROBE ISSUE

The automated tuning mechanism has developed a problem on the 1H channel. Until this probe is fixed, an interim double resonance probe i.e. 1H, 13C will be installed in AV301.

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DRX499 UPDATE : INSTRUMENT READY FOR USE

Users can block times as usual. The usual warnings and reminders highlighted last time when an incorrect sample insertion occurred, apply now also. Thank you for your cooperation.

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