UW CHEMISTRY NMR

Announcments & Equipment Logs

Spectrometer

GG500 – PLANNED MAINTENANCE , Jul. 1 Mon – IMPACT

For better part of the day on Jul. 1, Monday, the system will be down for hardware maintenance.  The automation queue will be stopped early in the morning that day.  Do not plan to queue any experiments from 8 AM. The Automation queue should resume from 5 PM latest, that day, but for unexpected contingencies. […]

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UPDATE : GG500 – SWITCH TO MANUAL MODE LATER TODAY

Due to the HVAC radiator maintenance and asbestos mitigation of the NMR lab yesterday,  the automation queue could not be continued from 4.30 pm. The system will attempt to complete the pending queue before it is switched to Topspin direct login. NMR Facility 6/18/24

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UPDATE ! GG500 – READY FOR AUTOMATION RUN – PLEASE QUEUE UP SAMPLES

Few reminders : You can download your data via the FTP server link:  phoenix.chem.washington.edu/GG500. You can set the temperature you desire, from the Automation Window itself.   The software will check the target temperature before starting the run A cumulative maximum of 60 minutes per sample holder position will be treated as a ‘walk-on’ run and […]

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NOTE ! GG500 – WILL ENTER ICONNMR AUTOMATION TOMORROW – FRI 14TH

The Topspin ICONNMR interface will be deployed starting noon tomorrow i.e. Friday, the 14th.   It is very similar to the NEO500 interface.  Here are points that are unique to GG500. Access : The system will be in Full IconNMR Automation mode from Friday morning 10 AM of a given week and continue till 10 AM […]

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UPDATE : NEO500 – READY FOR USE

The queue is started.  Please line up samples. NMR Facility

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GG500 : SYSTEM READY FOR USE – SAMPLE TUBE BREAKAGE FIXED

Based on what we observed,  a sample tube broke while a user loaded the sample with spinner into the Carousel.  This triggered an error condition of the Sample Robot. PLEASE PAY ATTENTION : With the Automation Hardware in place, we have reduced the physical human interaction with NMR machine to just a single step :  […]

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ALERT : GG500 – SAMPLE CHANGER ERROR

We are looking into the sample changer issue and will post an update as soon as it is resolved. NMR Services Manager 6/5/2024

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NEO500 USAGE PRACTICE – REMINDER

Like all instruments, NEO500 also has a walk-on usage policy where the software allows only a maximum of 60 minutes time during the day for a given sample.  The software automatically queues longer experiments to so-called ‘Night Mode’ and runs them overnight. We are hearing  that some users are stepping around this limitation by programming […]

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GG500 : FUNCTIONING NORMALLY

A software glitch was reported over the weekend and it has been resolved.  Instrument is functioning normally. NMR Services Manager 5/6/24

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UPDATE – NEO500 : ATMA issue resolved

Check the quality of your data if it was processed by the system before 3 pm today.  If it is not satisfactory,  please resubmit it. ATMA was non-functional until 2.45 pm.  But the default tune/match might have been good for some of the samples. If that’s the case, the data collected should be OK. NMR […]

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