UW CHEMISTRY NMR

Announcments & Equipment Logs

UPDATE ! AV301 – SYSTEM REVIVED FOR REGULAR USE

This is how the sample looked on top of the Probehead when User dropped it without spinner (WRONG !) _______________________________________________________ This is how it is SUPPOSED TO BE on top of the Probehead ( RIGHT !) Happy Friday ! NMR Facility Manager 2/28/20

Posted in Hardware, Spectrometer, Usage | No Comments

ALERT ! AV500 – SYSTEM DOWN…PNEUMATICS PROBLEM

Sample injection/ejection and spinning is not working.   Not sure if this is a simple fix or a delayed one as I write this.   Hunker down and wait for updates ! NMR Facility Manager 2/28/20

Posted in Hardware, Spectrometer | No Comments

ALERT ! AV301 NOT USABLE UNTIL TOMORROW…PLEASE READ

User has accidentally dropped a sample tube without the spinner turbine into the magnet. This means that the probehead has to be removed to remedy the situation, which will not happen until tomorrow morning. Until this is taken care of, the instrument is not usable.  The reservation calendar should reflect this and we will update […]

Posted in Hardware, Spectrometer | No Comments

UPDATE ! AV500 – LOGIN SYSTEM BACK TO NORMAL

You should be able to use your UWNetid as usual.  Thank you for patiently waiting this to be resolved. NMR Facility Manager 2/13/20

Posted in Host Computer, Operating System | No Comments

ALERT ! AV500 : AUTHENTICATION BROKEN (FOR A SHORT WHILE)

We are trying to do the needful so that your UWNetid login will start working again.  Until that work is done transparent to you,  you please use the following generic account : ‘genuser’  with its own magic  passphrase. Please construct the same from the phonetic equivalent I will type below. (As an example :  eM.oH.one.two.three will […]

Posted in Uncategorized | No Comments

UPDATE : FTP SERVER BACK TO NORMAL

If any of you noticed that the FTP server was not responding within the past 24 hours,  you will be glad to know that it is back to normal.   Please feel free to post a message in the online log book if you notice anything amiss. You can access all the log books from your […]

Posted in Datasets, Host Computer | No Comments

PLEASE NOTE ! NMR LAB DOOR CARD READER IS MALFUNCTIONING

I have left a wooden wedge to prop the door open as a temporary measure, since most of you may not have a physical key to open the door.  Please leave the wedge as it is, until we fix the door problem. Thank you NMR Facility Manager 2/12/2020

Posted in Usage | No Comments

ALERT ! AV301 : IMMINENT PROBE CHANGE

The automatic tuning/matching part seems to be malfunctioning for the X-channel on this probe.  We are planning to pull the probe out tomorrow afternoon i.e. Friday the 7th and see if its a quick fix. If this is not the case, then be prepared to say hello to the old fashion Broadband probe, that needs […]

Posted in Hardware, Spectrometer | No Comments

NOTE ! : DRX499 – (HOPEFULLY) USEFUL EMBELLISHMENT

Hello after a long break and Happy Wednesday and Happy New Year 2020 ! DRX499 Since we all still have to tune/match the TXO-19F,13C {1H} NMR probehead by hand by crouching under the magnet, we are throwing some light on the process.  We have provided a corded LED lamp to light up the probehead space under […]

Posted in Hardware, Spectrometer | No Comments

ALERT ! NMR RESERVATION SYSTEM SNAFU

Hello All As I write this, one or many of the reservation calendar for the NMR instruments might fail with a message similar to the following. The reservation server is causing this problem and until that gets resolved,  please record your usage on a plain paper with the following details and keep it next to […]

Posted in Host Computer, Operating System | No Comments

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