UW CHEMISTRY NMR

Announcments & Equipment Logs

ALERT: AV300 UNABLE TO RUN DUE TO TUNE ISSUES

Users: The av300 BBI probe has been misused again and is no longer tuning/matching on the 1H, which precludes proton and any 1H-decoupled-X-observe NMR. Until the NMR Managers can take a look, please do not run on the av300 because using the av300 in its current state risks further damage to the console. Please watch […]

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LOGIN ISSUES RESOLVED on AV300 and DRX499

Login issues have been resolved on both the av300 and drx499 spectrometers.

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ALERT ! : DRX499 – UWNETID LOGIN DOWN…TEMPORARILY

An issue similar to that of AV300 is not allowing users to login with their NetID currently. We are working on this and post an update as soon as the issue is resolved.  

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AV300 : USER LOGIN NOT WORKING

The UWNetid is not functional and we are working on this.  I will provide an alternative or any useful updates on the situation, shortly. NMR Facility Manager 11/16/15

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ATTENTION ! AV301 UPDATE : GRADIENTS AND TOPSHIM OPERATIONAL

The new gradient capability is fully functional.   Combined with the ATMA feature of the porbehead,  users can do everything from the computer desktop, including shimming using TOPSHIM.  PROBE TUNING :   After inserting sample and setting up the correct dataset, just enter atma on the command line.  Wait for the auto tuning/matching to complete. SHIMMING :    Topshim […]

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UPDATE ! AV301 – SYSTEM IS READY FOR REGULAR USE – GRADIENT UPGRADE INCOMPLETE

I apologize for this unexpected delay in implementing gradient upgrade but we hope the wait will be worth it, once users can let the computer do all the shimming.   I am glad to report that the major part of this hardware and software upgrade is done and I hope that by Thursday, the 12th, […]

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AV300: Back in Service

The BBI probe has been repaired and the av300 is now available for use. Thank you for your patience. Please notify a NMR Facility Manager with any further questions or concerns.

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AV300: 1H Tune Issue

The av300 is currently down due to an issue with the probe that occurs when users use fingers to tune or use the tune tool at an angle on the 1H tune rod. We are currently working to fix the probe and will notify users when the instrument is available again.

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AV301 UPGRADE MAINTENANCE: ON-GOING

Users: Please note that the av301 is still undergoing the upgrade maintenance and is not currently open for use. We will let you know when the instrument is available. Please see a NMR Facility Manager with any questions. Thank you for your patience.

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NOTE ON AV301 – PABBI PROBEHEAD AND SHIM

As already mentioned, the new gradient upgrade is designed to function with only the ATMA-BBI probe, as currently there are no other 300 MHz probes that feature gradient capability.  So, the probehead has been changed to PABBI and the probe ID card on the console lists the shim file to load and use along with the […]

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