UW CHEMISTRY NMR

Announcments & Equipment Logs

AV500 : ALERT : LOW VT SYSTEM NOT AVAILABLE

The LN2 evaporator assembly cracked open and it is being repaired as we speak.  Till that is ready,  users won’t be able to do a low VT run which requires LN2 evaporation.  We will post an update as soon as the system is operational in this regard.

Posted in Hardware, Spectrometer | No Comments

ALERT ! NMRJUCER DATA PROCESSING WORKSTATION IS BACK !

The NMRJuicer Data processing workstation has been rebuilt and tested and it is ready for use.  I thank the users for their immense patience during it’s absence. Here is a quick orientation on the salient features : Please use your UWNetid for login.  Once you login,  the Firefox web browser and the Topspin software automatically […]

Posted in Datasets, Host Computer, Operating System, Usage | No Comments

UPDATE : AV300 – SAMPLE SPINNER RECOVERED FROM MAGENT

Users are strongly advised to pay attention to the way they position sample tubes in the spinner before injecting in the magnet.  One person’s carelessness is going to cost NMR time to all the users. Thank you for your cooperation.

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AV700 – UPDATE : LOGIN ISSUES

We are working on the login issues mentioned yesterday by users.   In the meanwhile, a temporary solution is provided where users can login with a generic account and use the instrument.  Please contact either of the facility staff for credentials to use this account.

Posted in Software, Spectrometer, Usage | No Comments

AV700 – UPDATE : THE NEW BBO PROBE IS READY FOR USE.

Users can block time for this X – direct detect double resonance probe that includes Z-gradient capability.  Please note that the 1H sensitivity will be quite lower compared to that of a BBI probe and one should plan the experiments accordingly. Please ask one of us if you have questions.

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AV700 – UPDATE ! NEW BBO SOLUTIONS PROBE WILL BE READY FOR REGULAR USE SHORTLY

The 700 MHz instrument has a new BBO solutions probe installed that is capable of observing two nuclei at the same time.  This is a state of the art probehead with Z-gradient capability and it can reach sample temperatures of 110 C, for prolonged runs.  With the modern low VT system,  the samples can be […]

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NOTE – NMR RESERVATION SYSTEM INTERRUPTION ON SUNDAY, Jan 4th

Our IT support has announced a maintenance schedule on Jan 4th from 7.00 am to noon that will affect the NMR reservation server.  Users are encouraged to book their time before Sunday itself to circumvent this disruption.

Posted in Spectrometer, Usage | No Comments

UPDATE : NMR RESERVATION SYSTEM WORKING FINE

Users can try now to book time the usual way and report to us if there is anything amiss. Thank you for your help.

Posted in Host Computer, Operating System | No Comments

ALERT ! : NMR RESERVATION SERVER DOWN

The IT support is informed about the problem with the NMR reservation server.  Update will be posted about the progress made in due course.    

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UPDATE – NMRJUICER : Workstation is functional

Users can login with their UWNetid as before.   Thank you for your patience.  As an added appeal,  I will request you to refrain from rebooting the computer, especially as a way of expressing your frustration.  You might be causing more problems than you expected.

Posted in Host Computer, Operating System | No Comments

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