UW CHEMISTRY NMR

Announcments & Equipment Logs

Software

AV301 UPDATE : NEW AUTOMATED BROADBAND PROBE

The 19F probe has been compromised and will need extensive repairs. In place of the old probe, the new BBI probe is installed in the system. IMPORTANT NOTE : This is a new generation probehead that does NOT allow you to do manual tune/match i.e. WOBB. You must use the command ‘atma’  instead and the […]

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AV500 UPDATE : SYSTEM IS BACK TO NORMAL

Users can start reserving time at once and use the instrument. Thank you for your patience.

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AV500 UPDATE : BF1 SHIFT COMPLETE

The Base Frequency of the spectrometer is now reset to : 499.956572 MHz. Getting the line shape close to factory spec is still a work in progress. But, the current resolution achieved is comparable to the values with which we were operating prior to the frequency shift.  Existing user created parameter sets and the Bruker […]

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AV500 : PRINTING UPDATE

Users can now do both an ‘active screen’ dump to the printer as well as bring up XWINPLOT program and plot the spectra via that route.  Please post a comment in the log if you observe anything otherwise.

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AV500 : PLANNED PROBE CHANGE and B0 FIELD CHANGE

The X{1H} -Z grad BBO probe will be tested and installed on 26th Oct’12, Friday.  The probe optimization will be performed over the weekend and the probe should be ready for use by Monday, the 28th of Oct ’12.  Along with this operation, the B0 field will be readjusted to re-position the LOCK field to […]

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AV500: Automation Scripts Functional

All the stock Bruker au programs, such as multizg, multi_zgvt, multi_zgvd, etc.  are operational once again. If users have their own au scripts, they should compile automatically, the first time you invoke them.   If you face any difficulty, please contact the facility manager.

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AV500 : automation scripts not working

Familiar automation scripts such as ‘xaua’ are not functioning as expected.  This is being looked into.  Please use workarounds that are viable. For instance, ‘xaua’ can be replaced with ‘rga’ followed by ‘zg’.   Please contact facility staff for assistance with this.

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AV300, AV500: PRINTING OK

The long standing problem of not able to print spectra from either the Topspin window or with the xwinPlot, plot editor program is now resolved. For routine use, you can use Ctrl-P  to print whatever is displayed in a active Topspin window to the printer, without the necessity of starting the plot editor.  

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AV300 : SYSTEM READY FOR USE

The system is ready to go.  Due to an ‘operator error’  i.e. oversight from myself, the reservation calendar was blocked till now.  That is taken care of and users can book the times as usual.  Sorry for the inconvenience caused.

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DRX499 : Spectrometer Operational

The failing acquisition issue is now rectified. Please keep the facility staff posted if you observe similar occurrence again.

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